(苯基亚磺酰)(苯磺酰基)甲烷合成路线 (共 6 条)
反应条件
piperidine; hydrogenchloride 1.) toluene, acetonitrile, room temperature, overnight, 2.) ethyl acetate; Multistep reaction;
参考文献
Jackson, Richard F. W.; Standen, Stephen P.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 2 p. 149 - 156
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
1.) 0 deg C, 1 h, 2.) 0 deg C to room temperature, 1.5 h;
参考文献
Nantz, M. H.; Radisson, X.; Fuchs, P. L.
Synthetic Communications, 1987 , vol. 17, # 1 p. 55 - 70
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=-20°C; 3 h;
参考文献
Jackson, Richard F. W.; Standen, Stephen P.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 2 p. 149 - 156
参考文献
Hinsberg
Journal fuer Praktische Chemie (Leipzig), 1912 , vol. <2> 85, p. 339
Journal fuer Praktische Chemie (Leipzig), 1913 , vol. 88, p. 54
反应条件
piperidine; hydrogenchloride
1.) toluene, acetonitrile, room temperature, overnight, 2.) ethyl acetate; Multistep reaction;
参考文献
Jackson, Richard F. W.; Standen, Stephen P.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 2 p. 149 - 156
参考文献
Breslow,R.; Mohacsi,E.
Journal of the American Chemical Society, 1962 , vol. 84, p. 684 - 685