in acetonitrile Ambient temperatureelectrochemical synthesis: divided cell, Pt plate electrodes, -2.30 V vs Ag/Ag(+), <Et4N>OTs as supporting electrolyte and <Bu4N>I as an anodic depolarizer;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 15 p. 1873 - 1877
Morton; Hechenbleikner
Journal of the American Chemical Society, 1936 , vol. 58, p. 1699
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Morton; Le Fevre; Hechenbleikner
Journal of the American Chemical Society, vol. 58, p. 755,757
sodium; pentane beim Einleiten von CO2 in das Reaktionsgemisch bei 37-38grad;
参考文献
Morton; Hechenbleikner
Journal of the American Chemical Society, 1936 , vol. 58, p. 1699
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Morton; Le Fevre; Hechenbleikner
Journal of the American Chemical Society, 1936 , vol. 58, p. 754
in neat (no solvent) (C2H5)3SiH and n-C6H13Cl in presence of AlCl3 at room temp.; vigorous react.;;
参考文献
Whitmore, F. C.; Pietrusza, E. W.; Sommer, L. H.
Journal of the American Chemical Society, 1947 , vol. 69, p. 2108 - 2110
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Gmelin Handbook: Si: MVol.C, 34, page 106 - 108