N-hexadecyl-N,N,N-trimethylammonium bromide; hydroxocobalamine hydrochloride in pentan-1-ol; water T=25°C; Addition; reduction; elimination; dimerization; 3 h; Electrolysisirradiation with visible light; Title compound not separated from byproducts;
参考文献
Gao, Jianxin; Rusling, James F.; Zhou, De-Ling
Journal of Organic Chemistry, 1996 , vol. 61, # 17 p. 5972 - 5977
in tetrahydrofuran addn. of Me3SnNa in THF to a soln. of 2-bromooctane in THF at 0°C under Ar; quenching after 1 h with a large excess H2O2, extg. (pentane), washing of extracts (H2O), drying (Na2SO4), GLPC;
参考文献
Journal of the American Chemical Society, , vol. 107, # 2 p. 416 - 423
