in N-dodecane excess of Me3Al in dodecane adding to suspn. of anhyd. Zn acetate in dodecane at room temp.; mixt. distg. through a 40 cm vigreux column and product collecting in toluene; identified by b. p.;
参考文献
Journal of Organometallic Chemistry, , vol. 225, # 1 p. 71 - 85
in gaseous matrix components vaporization into He, mixt. diln. further with He or H2, equilibration within 20 s in IR cell; IR spectroscopic monitoring;
参考文献
Journal of Physical Chemistry B, , vol. 101, # 25 p. 4882 - 4888
in neat (no solvent) (exclusion of moisture); co-condensation of MeZnBH4 and NH3, maintainingthe mixture at -78°C for ca. 24 h, removal of excess NH3 at -78. degree.C, slow warming to room temp. under continuous pumping; elem. anal.;
参考文献
Journal of the Chemical Society - Dalton Transactions, , # 6 p. 853 - 859
in gaseous matrix components vaporization into He, mixt. diln. further with He or H2, equilibration within 20 s in IR cell; IR spectroscopic monitoring;
参考文献
Journal of Physical Chemistry B, , vol. 101, # 25 p. 4882 - 4888
Justus Liebigs Annalen der Chemie, , vol. 111, p. 57
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, , p. 413
