n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=25°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Loewenthal, H. J. E.
Journal of the Chemical Society, Chemical Communications, 1990 , # 10 p. 768 - 769
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=25°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Loewenthal, H. J. E.
Journal of the Chemical Society, Chemical Communications, 1990 , # 10 p. 768 - 769
1: carbon disulfide; ethanol With sodium hydride T=20°C; 2 h; 2: methyl (R,S)-2-bromopropionate in ethanol 15 h; Heating; Further stages.;
参考文献
Brown, Steven L.; Rayner, Christopher M.; Graham, Susan; Cooper, Andrew; Rannard, Steven; Perrier, Sebastien
Chemical Communications, 2007 , # 21 p. 2145 - 2147