54509-73-8合成路线 （共 3623 条）
反应条件
methylalumoxane (PMAO-S) in toluene T=80°C; P=15001.5 Torr; 1 h; Product distribution / selectivity;
参考文献
US2007/27350 A1, ;
Page/Page column 7-8 ;
反应条件
1: With tri(n-octyl)aluminium in toluene T=80°C; 2: With CrCl3(THF)3; bis(di{ortho-methoxyphenyl}phosphanyl)(methyl)amine in toluene T=80°C; 1 h; Product distribution / selectivity;
参考文献
US2006/293546 A1, ;
Page/Page column 6-7 ;
反应条件
1: With [(t-Bu)NP(Ph)2N(t-Bu)]Cr(μ2-Cl)2Li(THF)2 in toluene T=60°C; P=26252.6 Torr; 1 h; Inert atmosphere; 2: With hydrogenchloride in ethanol; toluene
参考文献
Organometallics, , vol. 30, # 12 p. 3346 - 3352
反应条件
MAO; N,N-bis(1H-benzimidazol-2-ylmethyl)-N-methylamine Cr(III)Cl3 in toluene T=50°C; P=3000.24 Torr; 1 h; Product distribution; Further Variations:CatalystsPressures;
参考文献
Journal of the American Chemical Society, , vol. 128, # 24 p. 7704 - 7705
反应条件
(Ph2PN-(Me)(CH2)2-NPPh2)CrCl3(THF) in toluene T=80°C; P=30003 Torr; 0.5 h;
参考文献
Organometallics, , vol. 31, # 21 p. 7427 - 7433,7
反应条件
1: With [(t-Bu)NP(Ph)2N(t-Bu)]Cr(μ2-Cl)2Li(THF)2 in toluene T=100°C; P=26252.6 Torr; 1 h; Inert atmosphere; 2: With hydrogenchloride in ethanol; toluene
参考文献
Organometallics, , vol. 30, # 12 p. 3346 - 3352
反应条件
in dichloromethane T=-78°C;
参考文献
Brookhart, M.; Humphrey, M. B.; Kratzer, H. J.; Nelson, G. O.
Journal of the American Chemical Society, 1980 , vol. 102, # 26 p. 7802 - 7803
反应条件
in toluene T=20°C; 1.25 h;
参考文献
Palacios, Laura; Miao, Xiaowei; Di Giuseppe, Andrea; Pascal, Simon; Cunchillos, Carmen; Castarlenas, Ricardo; Perez-Torrente, Jesus J.; Lahoz, Fernando J.; Dixneuf, Pierre H.; Oro, Luis A.
Organometallics, 2011 , vol. 30, # 19 p. 5208 - 5213
反应条件
hydrogenchloride; dibenzoyl peroxide T=100°C; P=294203 - 367754 Torr;
参考文献
Journal of the American Chemical Society, , vol. 74, p. 4323
US2418832 , ;
US2440801 , ;
反应条件
hydrogen; acetic acid; [{Rh(μ-Cl)(1,5-cyclooctadiene)}2]; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt; diethylamine in water; toluene T=59.84°C; 6 h;
参考文献
COUNCIL OF SCIENTIFIC and INDUSTRIAL RESEARCH
Patent: WO2005/63668 A1, 2005 ;
Location in patent: Page/Page column 7-8 ;
