54509-73-8合成路线 (共 3623 条)
反应条件
N,N-dicyclohexylmethylamine; palladium diacetate; tetra-(n-butyl)ammonium iodide; [(t-Bu)3PH]BF4 in methanol; toluene T=130°C; Heck Reaction; P=7500.75 Torr; 0.333333 h;
参考文献
Bourne, Samuel L.; O'Brien, Matthew; Kasinathan, Sivarajan; Koos, Peter; Tolstoy, Paeivi; Hu, Dennis X.; Bates, Roderick W.; Martin, Benjamin; Schenkel, Berthold; Ley, Steven V.
ChemCatChem, 2013 , vol. 5, # 1 p. 159 - 172
反应条件
potassium carbonate; benzyltrioctylammonium chloride; bis(benzonitrile)palladium(II) dichloride in benzene T=160°C; P=7600 Torr; 2 h;
参考文献
Miura, Masahiro; Hashimoto, Hideo; Itoh, Kenji; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2207 - 2211
反应条件
sodium acetate; bis(dibenzylideneacetone)-palladium(0) in dichloromethane; acetone 2 h; Ambient temperature;
参考文献
Kikukawa, K.; Nagira, K.; Wada, F.; Matsuda, T.
Tetrahedron, 1981 , vol. 37, p. 31 - 36
参考文献
Kawamoto,K. et al.
Bulletin of the Chemical Society of Japan, 1971 , vol. 44, p. 1239 - 1243
反应条件
Co/C in tetrahydrofuran T=150°C; P=53203.6 Torr; 72 h;
参考文献
Chemical Communications (Cambridge, United Kingdom), , # 12 p. 1310 - 1311
参考文献
Union Carbide Corp.
Patent: US2851473 , 1955 ;
反应条件
dibenzoyl peroxide P=44130.5 Torr;
参考文献
Ziegler
Patent: DE864866 , 1950 ;
反应条件
N-bromosuccinmide; zirconium acetylacetonate; Co(OCOCH3)2; oxygen; potassium bromide in acetic acid T=20°C; P=912 - 1140 Torr; synergistic effect of catalyst components; MechanismRate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 24, # 10 p. 1854 - 1861
Zhurnal Organicheskoi Khimii, , vol. 24, # 10 p. 2056 - 2065
反应条件
Yield given. Multistep reaction;
参考文献
Hegedus,L.S.; Williams,R.E.; Mcguire,M.A.
Journal of the American Chemical Society, 1980 , vol. 102, p. 4973
参考文献
Justus Liebigs Annalen der Chemie, , vol. 567, p. 195,202