54509-73-8合成路线 （共 3623 条）
反应条件
aniline; aluminium anilide T=300 - 350°C; P=110326 - 147102 Torr;
参考文献
Ethyl Corp.
Patent: US2814646 , 1954 ;
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Farbenfabr.Bayer.
Patent: DE951501 , 1956 ;
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Farbenfabr.Bayer.
Patent: US2762845 , 1954 ;
反应条件
aluminium trichloride T=80°C; P=3677.5 Torr; Hydrogenation.und Erhitzen der bei 190-195grad siedenden Anteile des nach dem Behandeln mit wss.Natriumcarbonat-Loesung erhaltenen Reaktonsprodukts mit wss.Ammoniak und Kupfer(I)-oxid auf 225grad;
参考文献
Dow Chem.Co.
Patent: US2159370 , 1937 ;
反应条件
T=330°C; P=25742.8 Torr;
参考文献
Ecke et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 639,641
反应条件
T=330°C; P=29420.3 - 33097.9 Torr; 9-stdg.;
参考文献
Ecke et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 639,641
反应条件
trifluorormethanesulfonic acid; tetra-(n-butyl)-phosphonium bromide; triphenylphosphine; PtBr2 T=150°C; 10 h; AutoclaveHigh pressureSchlenk techniqueInert atmosphere; Catalytic behavior;
参考文献
Bethegnies, Aurelien; Dub, Pavel A.; Poli, Rinaldo
Organometallics, 2013 , vol. 32, # 6 p. 1882 - 1891
反应条件
silver tetrafluoroborate; dibromo[1,3-dihydro-1-(2-pyridinyl)-3-(2,4,6-trimethylphenyl)-2H-imidazol-2-ylidene]platinum(II) in PhNO2-d5 T=20 - 150°C; P=4125.41 Torr; 26 h; Inert atmosphere;
参考文献
Cao, Peng; Cabrera, Jose; Padilla, Robin; Serra, Daniel; Rominger, Frank; Limbach, Michael
Organometallics, 2012 , vol. 31, # 3 p. 921 - 929
反应条件
T=500°C; P=220652 Torr;
参考文献
O'Kelly; Sachanen
Industrial and Engineering Chemistry, 1946 , vol. 38, p. 467
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Schmerling in B.T.Brooks et al.
The Chemistry of Petroleum Hydrocarbons,Bd.III <New York 1955> S.368
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Socony-Vacuum Oil Co.
Patent: US2410107 , 1943 ;
反应条件
T=0 - 5°C; P=7355.08 Torr; Produkt 5: 2.3-Dimethyl-pentan; Produkt 6: 2.4-Dimethyl-pentan; Produkt 7: Octan; Produkt 8: Nonan;
参考文献
Schmerling
Journal of the American Chemical Society, 1945 , vol. 67, p. 1778
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Koch; Richter
Chemische Berichte, 1944 , vol. 77/79, p. 128
反应条件
T=59.9344°C; P=20686.5 Torr; 0.5 h; Product distribution / selectivity;
参考文献
Randolph, Bruce B.; Kimble, James B.; Johnson, Marvin M.
Patent: US2004/10175 A1, 2004 ;
Location in patent: Page 9-10 ;
反应条件
T=34.7678°C; P=20686.5 Torr; 0.5 h; Product distribution / selectivity;
参考文献
Randolph, Bruce B.; Kimble, James B.; Johnson, Marvin M.
Patent: US2004/10175 A1, 2004 ;
Location in patent: Page 17-18 ;
