54509-73-8合成路线 (共 3623 条)
参考文献
Zhurnal Obshchei Khimii, , vol. 5, p. 537,539,542
Chem. Zentralbl., , vol. 106, # II p. 3090
Gazzetta Chimica Italiana, , vol. 64, p. 54
反应条件
copper(l) chloride; silicon in toluene T=159.9°C; P=3040 Torr; 3 h; also ethanol; other solvents; effect of the amount of methanol on the silicon conversion and selectivity for organomethoxysilanes; var. pressures, times and temperatures; Product distributionMechanism;
参考文献
Okamoto, Masaki; Watanabe, Naoto; Suzuki, Eiichi; Ono, Yoshio
Journal of Organometallic Chemistry, 1995 , vol. 489, # 1-2 p. C12 - C16
反应条件
Pt(0) hexavinyldisiloxane complex T=60 - 70°C; 1.5 h; Title compound not separated from byproducts.;
参考文献
Russian Journal of General Chemistry, , vol. 76, # 2 p. 225 - 228
反应条件
in benzene T=82°C; Cycloaddition; Diels-Alder reaction; 48 h;
参考文献
Papavassiliou; Mousdis; Papadima
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2000 , vol. 55, # 2 p. 231 - 232
反应条件
Fe(acac)3; TEA; triethylaluminum in toluene T=70°C; P=3000240 Torr; 1.5 h; Product distribution; Further Variations:TemperaturesPressuresreagents ratio;
参考文献
Belova; Matkovskii
Petroleum Chemistry, 2002 , vol. 42, # 2 p. 110 - 120
反应条件
di-tert-butyl peroxide T=140°C; 0.5 h; variation of educt-ratio, ratio of rate constants of addition of acyl radical to decarbonylation; Product distributionMechanism;
参考文献
Orlova, S. V.; Ikonnikov, N. S.; Terent'ev, A. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 6 p. 1222 - 1225
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 6 p. 1356 - 1360
反应条件
Mo(tfd)2(bdt) in chloroform; acetonitrile-D3 22.325 h; Reflux;
参考文献
Harrison, Daniel J.; Fekl, Ulrich
Chemical Communications, 2009 , # 48 p. 7572 - 7574
反应条件
T=250°C; P=53692.1 Torr; Produkt5:Butyl-sek.-butyl-aether; Produkt6:Butyl-tert.-butyl-aether; Produkt7:sek.-Butylalkohol; Produkt8:Diaethylaether;
参考文献
Newitt; Semerano
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1936 , vol. 157, p. 354
反应条件
aluminium trichloride; toluene
参考文献
Lippmann
Justus Liebigs Annalen der Chemie, 1864 , vol. 129, p. 85
反应条件
(i) PdCl2, benzene, (ii) /BRN= 3587209/; Multistep reaction;
参考文献
Tsuji,J. et al.
Tetrahedron Letters, 1963 , p. 1061 - 1064