54509-73-8合成路线 （共 3623 条）
反应条件
T=-60°C; und anschliessend mit CO2;
参考文献
Bartlett et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 1771
反应条件
AlCl3, aluminium chloride; sodium chloride in dichloromethane 2 h; Cooling with ice;
参考文献
FUJITSU LIMITED; Kamiya, Nozomu; Tomonaga, Atsushi; Sugiyama, Hajime
Patent: US2013/317110 A1, 2013 ;
Location in patent: Paragraph 0140 ;
反应条件
pyridine; dicobalt octacarbonyl T=160°C; P=90009 Torr; 2.5 h; Kinetics;
参考文献
SASOL TECHNOLOGY (PROPRIETARY) LIMITED
Patent: WO2008/23338 A1, 2008 ;
Location in patent: Page/Page column 22; sheet 9/11 ;
反应条件
1: in toluene T=20 - 116°C; P=26252.6 - 42004.2 Torr; 2.33333 h; 2: With sulfuric acid; water T=40°C;
参考文献
WO2005/123639 A1, ;
Page/Page column 10-11 ;
反应条件
1: in toluene T=20 - 116°C; P=17851.8 - 42004.2 Torr; 2 - 3 h; 2: With sulfuric acid; water T=40°C; Product distribution / selectivity;
参考文献
WO2005/123639 A1, ;
Page/Page column 8-9 ;
反应条件
KrF laser induced telomerization; KineticsRate constant;
参考文献
Linyang; Fuss; Kompa
Berichte der Bunsengesellschaft/Physical Chemistry Chemical Physics, 1990 , vol. 94, # 8 p. 874 - 882
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=120°C; P=22800 Torr; 24 h;
参考文献
Izumi, Taeko; Nishimoto, Yasuhiro; Kohei, Kunihiro; Kasahara, Akira
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1419 - 1424
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=120°C; P=22800 Torr; 24 h;
参考文献
Izumi, Taeko; Nishimoto, Yasuhiro; Kohei, Kunihiro; Kasahara, Akira
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1419 - 1424
反应条件
tetrabutylammomium bromide in dichloromethane T=80°C; 7 h; other nucleophiles possible (NaN3, NaNO2, KSCN, KCN), other solvents possible (C2H4Cl2, ethyl acetate);
参考文献
Rozhkov, I. N.; Igumnov, S. M.; Pletnev, S. I.; Chaplina, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 4.2 p. 856
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 4 p. 951
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=120°C; P=22800 Torr; 24 h;
参考文献
Kasahara, Akira; Izumi, Taeko; Murakami, Satoshi; Miyamoto, Kazuhiro; Hino, Toshimi
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1405 - 1413
