54509-73-8合成路线 （共 3623 条）
反应条件
in n-heptane under argon, EtAlCl2, Al powder and n-heptane are heated to 120°C in an autoclave under stirring, ethylene is pressed on for 120 h; filtn., filtrate is distd. in high vac. at 100°C; elem. anal.;
参考文献
Martin, Heinz; Bretinger, Helmut
Zeitschrift fuer Naturforschung, Teil B: Chemical Sciences, 1991 , vol. 46, p. 615 - 620
反应条件
in n-heptane byproducts: (CH2CHCHCH2CH(CH3))x; High Pressure; (Ar); to a soln. of Al-compound and Al added ethylene (20 bar pressure) under stirring at 100-150°C for 16 h; distd. in vacuo at 50°C; elem. anal.;
参考文献
Martin, Heinz; Bretinger, Helmut
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 2 p. 182 - 186
参考文献
Botteron,D.G.; Shulman,G.P.
Journal of Organic Chemistry, 1962 , vol. 27, p. 1059 - 1061
反应条件
(10H)-phenothiazine; bis(.mu.-chloro)bis{(2-(1-(hydroxyimino)methyl)phenyl-C1,N)palladium(II)}; potassium acetate in N,N-dimethyl acetamide T=105°C; Heck-Mizoroki reaction; P=775.743 Torr; 6 h; Inert atmosphere;
参考文献
Smith, Craig R.; RajanBabu
Tetrahedron, 2010 , vol. 66, # 5 p. 1102 - 1110
反应条件
MCM-22 T=176.7 - 204.4°C; P=12901.3 Torr; 600 h; Product distribution / selectivity;
参考文献
Brown, Stephen H.; Collins, Nick A.
Patent: US2008/194896 A1, 2008 ;
Location in patent: Page/Page column 10-11 ;
反应条件
hydrogenchloride in water; acetonitrile T=5 - 10°C; P=45003.6 Torr; electrolysis, further solvent methanol;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 3 p. 523 - 525
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 582 - 584
反应条件
hydrogenchloride in methanol T=5 - 10°C; P=45003.6 Torr; electrolysis, further solvent aq. acetonitrile;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 3 p. 523 - 525
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 582 - 584
参考文献
Irwin; Hennion
Journal of the American Chemical Society, 1941 , vol. 63, p. 859
反应条件
1,4-dioxane; polyethylene glycol chlorohydrin; chlorine; 2-chloro-ethanol T=25 - 35°C;
参考文献
Reppe,W.
Acetylene Chemistry <New York 1949> S.19
Full Text Show Details
Schilow; Kanjajew
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 109
Chem.Abstr., 1948 , p. 4127
Full Text Show Details
Dow Chem.Co.
Patent: US2095612 , 1934 ;
反应条件
hydrogenchloride T=5 - 10°C; P=45003.6 Torr; electrolysis;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 3 p. 523 - 525
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 582 - 584
