54509-73-8合成路线 (共 3623 条)
反应条件
oxygen in gas P=30 Torr; flame stabilized diffusion, analysed by MS; Mechanism;
参考文献
Bastin, Eric; Delfau, Jean-Louis; Reuillon, Marcelline; Vovelle, Christian
Journal de Chimie Physique et de Physico-Chimie Biologique, 1987 , vol. 84, # 3 p. 415 - 420
反应条件
in toluene T=225°C; 1.5 h;
参考文献
Takeshita, Hitoshi; Hatsui, Toshihide; Shimooda, Isao; Mametsuka, Hiroaki
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 7 p. 2291 - 2292
反应条件
dibenzoyl peroxide T=100°C; Product distributionMechanism;
参考文献
Dzheiranishvili, M. S.; Levinskii, M. B.; Chkhubianishvili, N. G.; Afanas'ev, I. B.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 445 - 447
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 3 p. 516 - 518
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9-10 ;
反应条件
(i), (ii) MeMgHal; Multistep reaction;
参考文献
Freidlina,R.Kh. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1961 , p. 1168 - 1171
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , # 7 p. 1256 - 1261
反应条件
T=300°C; P=29420.3 Torr;
参考文献
Montclair Research Corp. und Ellis-Foster Co.
Patent: US2721873 , 1952 ;
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 708,709
Chem.Abstr., 1952 , p. 7514
参考文献
Movsumzade,M.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1972 , vol. 8, p. 2077 - 2079
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, # 10 p. 2031 - 2034
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 708,709
Chem.Abstr., 1952 , p. 7514