54509-73-8合成路线 （共 3623 条）
反应条件
ammonia; hydrogen; LaCaY; rhodium in gas
T=210°C; P=97507.8 Torr; 5 h; other initial pressures, other supports for Rh-catalyst (catalyst = 1 wt. percent Rh/support), effect of the nature of the support on the activity and selectivity of the Rh-catalyst; Product distributionKineticsMechanism;
参考文献
Kosolapova, B. S.; Levin, D. Z.; Sominskii, S. D.; Rar, L. F.; Mortikov, E. S.; Lapidus, A. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 11 p. 2244 - 2248
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 11 p. 2481 - 2486
反应条件
336 h; Ambient temperature; Product distributionMechanism;
参考文献
Maercker, Adalbert; Passlack, Michael
Chemische Berichte, 1983 , vol. 116, # 2 p. 710 - 723
反应条件
tri-ruthenium(0)dodecacarbonyl in benzene
T=150°C; P=29420.3 Torr; 4 h; Yield given. Yields of byproduct given;
参考文献
Tsuji, Yasushi; Ohsumi, Tatsuya; Kondo Teruyuki; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1986 , vol. 309, p. 333 - 344
反应条件
Yield given. Multistep reaction;
参考文献
Hegedus,L.S.; Darlington,W.H.
Journal of the American Chemical Society, 1980 , vol. 102, p. 4980
反应条件
tetrabutylammomium bromide; water; lithium perchlorate; niobium bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=0 - 5°C; P=760 Torr; The reaction was carried out by electrolysis.;
参考文献
Rollin, Y; Meyer, G.; Troupel, M.; Fauvarque, J. F.
Tetrahedron Letters, 1982 , vol. 23, # 35 p. 3573 - 3576
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in N,N-dimethyl-formamide
T=100 - 120°C; P=22501.8 Torr;
参考文献
Detert, Heiner; Sugiono, Erli
Advanced Synthesis and Catalysis, 1999 , vol. 341, # 4 p. 358 - 362
反应条件
N,N-dicyclohexylmethylamine; palladium diacetate; tetra-(n-butyl)ammonium iodide; [(t-Bu)3PH]BF4 in methanol; toluene
T=130°C; Heck Reaction; P=7500.75 Torr; 0.333333 h;
参考文献
Bourne, Samuel L.; O'Brien, Matthew; Kasinathan, Sivarajan; Koos, Peter; Tolstoy, Paeivi; Hu, Dennis X.; Bates, Roderick W.; Martin, Benjamin; Schenkel, Berthold; Ley, Steven V.
ChemCatChem, 2013 , vol. 5, # 1 p. 159 - 172
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in N,N-dimethyl-formamide
P=3750.3 Torr; var. of pressure; Product distribution;
参考文献
Detert, Heiner; Sugiono, Erli
Advanced Synthesis and Catalysis, 1999 , vol. 341, # 4 p. 358 - 362
反应条件
N-bromosuccinmide; bis(benzonitrile)palladium(II) dichloride
1) THF, a) 0 deg C, 10 min., b) -50 deg C, 50 min., 2) -50 deg C, 5 min., 2h RT; Yield given. Multistep reaction;
参考文献
Baeckvall, Jan E.; Bjoerkman, Eva E.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2893 - 2898
反应条件
(10H)-phenothiazine; bis(.mu.-chloro)bis{(2-(1-(hydroxyimino)methyl)phenyl-C1,N)palladium(II)}; potassium acetate in N,N-dimethyl acetamide
T=105°C; Heck-Mizoroki reaction; P=775.743 Torr; 10 h; Inert atmosphere;
参考文献
Smith, Craig R.; RajanBabu
Tetrahedron, 2010 , vol. 66, # 5 p. 1102 - 1110
