54509-73-8合成路线 (共 3623 条)
反应条件
methanesulfonic acid; Pd(OAc)2*1,2-bis(di-s-butylphosphino)ethane T=120°C; Product distribution; Further Variations:ratio Pd(OAc)2:ligand:CH3SO3H;
参考文献
Pugh, Robert I.; Drent, Eite
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 8 p. 837 - 840
反应条件
dodecacarbonyltetrarhodium(0) T=125°C; P=36775.4 Torr; 6 h; the influence of reaction temperature on product yield/distribution; Product distribution;
参考文献
Chemistry Letters, , p. 989 - 992
反应条件
tri-ruthenium(0)dodecacarbonyl; triethylamine T=160°C; P=11250.9 Torr; 24 h; var. catalysts, bases; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 240, # 2 p. 169 - 178
反应条件
cobalt catalyst in butanone T=160°C; 2.41667 h; Yield given;
参考文献
Budennyi, A. P.; Rybakov, V. A.; Gvozdovskii, G. N.; Shuleva, N. I.; Gavrilova, V. M.
J. Appl. Chem. USSR (Engl. Transl.), 1981 , vol. 54, # 4 p. 771 - 776,621 - 625
反应条件
[RhH(PEt3)4] T=110°C; Carbonylation; P=26252.6 Torr;
参考文献
Robertson, Ruth A. M.; Poole, Andrew D.; Payne, Marc J.; Cole-Hamilton, David J.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1817 - 1819
反应条件
T=220 - 250°C; P=485435 - 610471 Torr;
参考文献
BASF
Chem. Zentralbl., 1954 , vol. 125, p. 1587
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BASF
Patent: DE860350 ;
反应条件
T=150°C; P=95616 - 125036 Torr;
参考文献
Reppe; Magin
Patent: US2577208 , 1950 ;
反应条件
tris(triphenylphosphine)ruthenium(II) chloride T=210°C; 18 h; other aldehydes and olefines; Product distribution;
参考文献
Isnard, P.; Denise, B.; Sneeden, R. P. A; Cognion, J. M.; Durual, P.
Journal of Organometallic Chemistry, 1982 , vol. 240, # 3 p. 285 - 288
参考文献
Reppe; Vetter
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 135,148
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BASF
Patent: DE890942 , 1943 ;
Full Text Show Details
Reppe,W.
Acetylene Chemistry <New York 1949> S. 178
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BASF
Chem. Zentralbl., 1954 , vol. 125, p. 1395
反应条件
trimethylamine-N-oxide; [N(4-C6H4Br)3][B(C6F5)4]; triethylaluminum; [Cr(CO)4(2-C6H4(MeO))2PN(Me)P(2-C6H4(MeO))2] in toluene T=60°C; P=30002.4 Torr; 1 h;
参考文献
Bowen, Lucy E.; Haddow, Mairi F.; Orpen, A. Guy; Wass, Duncan F.
Dalton Transactions, 2007 , # 11 p. 1160 - 1168