54509-73-8合成路线 （共 3623 条）
反应条件
1,2-bis(3,5-dimethylpyrazol-1-ylmethyl)benzenenickel(II) bromide; ethylaluminum dichloride P=30402 Torr; 0.25 h; Inert atmosphereSchlenk technique; Catalytic behavior; TemperatureTimePressure;
参考文献
Budhai, Asheena; Omondi, Bernard; Ojwach, Stephen O.; Obuah, Collins; Osei-Twum, Emmanuel Y.; Darkwa, James
Catalysis Science and Technology, 2013 , vol. 3, # 12 p. 3130 - 3135
反应条件
ammonia; hydrogen; LaCaY; rhodium in gas T=210°C; P=97507.8 Torr; 5 h; other initial pressures, other supports for Rh-catalyst (catalyst = 1 wt. percent Rh/support), effect of the nature of the support on the activity and selectivity of the Rh-catalyst; Product distributionKineticsMechanism;
参考文献
Kosolapova, B. S.; Levin, D. Z.; Sominskii, S. D.; Rar, L. F.; Mortikov, E. S.; Lapidus, A. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 11 p. 2244 - 2248
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 11 p. 2481 - 2486
反应条件
in toluene P=45600 Torr; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Chemical Research, Miniprint, , # 10 p. 2601 - 2623
反应条件
trimethylamine-N-oxide 1.) petroleum ether, RT, 4 h, 2.) toluene, MeOH, from 25 to 30 atm, 40 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 52, # 21 p. 7391 - 7420
反应条件
oxygen; tri-ruthenium(0)dodecacarbonyl in benzene T=130°C; P=7600 Torr; 6 h; effects of various catalysts, pressures; Product distribution;
参考文献
Bulletin de la Societe Chimique de France, , vol. 132, p. 609 - 614
反应条件
mercury dichloride in further solvent(s) 45-50h shaking at 350-400Torr; dry HgCl2, dry piperidine;;
参考文献
Chatt
Chemical Reviews (Washington, DC, United States), 1951 , vol. 48, p. 7
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Gmelin Handbook: Hg: MVol.B2, 114, page 637 - 640
反应条件
potassium carbonate; benzyltrioctylammonium chloride; bis(benzonitrile)palladium(II) dichloride in benzene T=160°C; P=7600 Torr; 2 h;
参考文献
Miura, Masahiro; Hashimoto, Hideo; Itoh, Kenji; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2207 - 2211
反应条件
(10H)-phenothiazine; bis(.mu.-chloro)bis{(2-(1-(hydroxyimino)methyl)phenyl-C1,N)palladium(II)}; potassium acetate in N,N-dimethyl acetamide T=105°C; Heck-Mizoroki reaction; P=1551.49 Torr; 24 h; Inert atmosphere;
参考文献
Smith, Craig R.; RajanBabu
Tetrahedron, 2010 , vol. 66, # 5 p. 1102 - 1110
反应条件
sodium acetate; bis(dibenzylideneacetone)-palladium(0) in dichloromethane; acetone 2 h; Ambient temperature;
参考文献
Kikukawa, K.; Nagira, K.; Wada, F.; Matsuda, T.
Tetrahedron, 1981 , vol. 37, p. 31 - 36
反应条件
byproducts: C2H6, H2, sulfur; Irradiation (UV/VIS); with six to ten fold H2S excess;
参考文献
Gmelin Handbook: S: SVol.4a/b, 1.3.11.2, page 291 - 298
