1,4-二硫杂螺[4.5]癸-8-基苯甲酸酯合成路线 （共 7 条）
反应条件
potassium hydroxide in methanol 3 h; Heating;
参考文献
Meyer, Walter L.; Brannon, Michael J.; Burgos, Celmira da G.; Goodwin, Thomas E.; Howard, Ralph W.
Journal of Organic Chemistry, 1985 , vol. 50, # 4 p. 438 - 447
反应条件
sodium methylate in methanol 15 h; Heating;
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
反应条件
1: 82 percent / chromium trioxide / acetic acid; H2O
2: 92 percent / toluene-p-sulphonic acid / benzene / Heating
View Scheme
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
反应条件
1: 60.8 percent / pyridine / CHCl3 / 5 h / 0 - 5 °C
2: 82 percent / chromium trioxide / acetic acid; H2O
3: 92 percent / toluene-p-sulphonic acid / benzene / Heating
View Scheme
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
反应条件
1: 100 percent / aq. KOH / methanol / 3 h / Heating
2: 100 percent / 99percent dicyclohexylcarbodiimide, H3PO4 / dimethylsulfoxide; benzene / 3 h
View Scheme
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
反应条件
in tetrahydrofuran
1 h; Heating;
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
