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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
钛酸四异丙酯
合成路线
（共 130 条）
546-68-9
钛酸四异丙酯
+
814-67-5
1,2-丙二硫醇
→
反应条件
126975-32-4
+
67-63-0
异丙醇
反应条件
in benzene N2-atmosphere; azeotropic distn. of i-ProH, evapn. (reduced pressure), trituration of residue (petroleum ether), filtration, drying (vac.);
参考文献
Jones, J.; Douek, J. A.
Polyhedron, 1989 , vol. 8, p. 2893 - 2896
546-68-9
钛酸四异丙酯
+
496-74-2
甲苯-3,4-二硫酚
→
反应条件
126975-34-6
+
67-63-0
异丙醇
反应条件
in benzene N2-atmosphere; azeotropic distn. of i-PrOH, evapn. (reduced pressure), repeated dissoln. in petroleum, evapn. (reduced pressure);
参考文献
Jones, J.; Douek, J. A.
Polyhedron, 1989 , vol. 8, p. 2893 - 2896
546-68-9
钛酸四异丙酯
+
75-91-2
叔丁基过氧化氢
→
反应条件
247235-00-3
+
67-63-0
异丙醇
反应条件
in dichloromethane Kinetics; room temp.;; FTIR;
参考文献
Finn; Sharpless, K. Barry
Journal of the American Chemical Society, 1991 , vol. 113, # 1 p. 113 - 126
546-68-9
钛酸四异丙酯
+
4198-93-0
→
反应条件
反应条件
in dichloromethane Kinetics; room temp.; FTIR;
参考文献
Finn; Sharpless, K. Barry
Journal of the American Chemical Society, 1991 , vol. 113, # 1 p. 113 - 126
546-68-9
钛酸四异丙酯
+
540-63-6
→
反应条件
27244-92-4
+
67-63-0
异丙醇
反应条件
in benzene N2-atmosphere; azeotropic distn. of i-PrOH, evapn. (reduced pressure), trituration of residue (petroleum ether), filtration, drying (vac.);
参考文献
Jones, J.; Douek, J. A.
Polyhedron, 1989 , vol. 8, p. 2893 - 2896
546-68-9
钛酸四异丙酯
+
107-21-1
→
反应条件
反应条件
暂无反应条件数据
参考文献
SHISEIDO COMPANY, LTD.
Patent: EP1930337 A1, 2008 ;
Location in patent: Page/Page column 11 ;
546-68-9
钛酸四异丙酯
→
反应条件
108-20-3
反应条件
in gas byproducts: CH3CHCH2; decomposition at a pressure of ca. 0.01 mm of Hg at 550°C; further compound: H2 was obtained with a yield of <0.5percent; org. compounds collected in a liquid-N2 trap; NMR; GC; mass spectra;
参考文献
Inorganic Chemistry, , vol. 29, p. 3065 - 3066
124-07-2
+
546-68-9
钛酸四异丙酯
→
反应条件
反应条件
Kinetics; Octanoic acid is added dropwise to titanium tetraisopropoxide under nitrogen.; Reaction is conducted under N2.;
参考文献
Riman; Landham; Bowen
Journal of the American Ceramic Society, 1989 , vol. 72, # 5 p. 821 - 826
546-68-9
钛酸四异丙酯
+
802294-64-0
→
反应条件
反应条件
Kinetics; Propanoic acid is added dropwise to titanium tetraisopropoxide under nitrogen.; Reaction is conducted under N2.;
参考文献
Riman; Landham; Bowen
Journal of the American Ceramic Society, 1989 , vol. 72, # 5 p. 821 - 826
112-80-1
+
546-68-9
钛酸四异丙酯
→
反应条件
反应条件
Kinetics; Oleic acid is added dropwise to titanium tetraisopropoxide under nitrogen.; Reaction is conducted under N2.;
参考文献
Riman; Landham; Bowen
Journal of the American Ceramic Society, 1989 , vol. 72, # 5 p. 821 - 826
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