三丁基(2-噻吩基)锡合成路线 (共 133 条)
反应条件
trans-dichloro(1,3-bis-(2,6-diisopentylphenyl)imidazolylidinium)(3-chloro-pyridine); cesium fluoride in 1,4-dioxane T=20 - 80°C; Stille-Migita cross-coupling; 24 h; Molecular sieveInert atmosphere;
参考文献
Dowlut, Meenakshi; Mallik, Debasis; Organ, Michael G.
Chemistry - A European Journal, 2010 , vol. 16, # 14 p. 4279 - 4283
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=90°C; Stille reaction;
参考文献
Hu, Zhaokang; Reichmanis, Elsa
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 5 p. 1155 - 1162
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); cesium fluoride in N,N-dimethyl-formamide T=45°C; Stille reaction; 1 h;
参考文献
Mee, Simon P. H.; Lee, Victor; Baldwin, Jack E.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 9 p. 1132 - 1136
反应条件
PhCH2Pd(PPh3)2Cl in toluene Heating;
参考文献
Sosabowski, Michael H.; Powell, Paul
Journal of Chemical Research, Miniprint, 1997 , # 1 p. 201 - 219
反应条件
palladium diacetate in tetrahydrofuran T=20°C; Stille reaction; 1.5 h;
参考文献
Synthesis, , # 7 p. 1117 - 1122
反应条件
palladium dichloride in acetonitrile T=20°C; 3 h;
参考文献
Synthetic Communications, , vol. 31, # 7 p. 1027 - 1034
反应条件
trans-dichloro(1,3-bis-(2,6-diisopentylphenyl)imidazolylidinium)(3-chloro-pyridine); cesium fluoride in 1,4-dioxane T=20 - 80°C; Stille-Migita cross-coupling; 24 h; Molecular sieveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 14 p. 4279 - 4283
反应条件
tris-(dibenzylideneacetone)dipalladium(0); copper(I) bromide dimethylsulfide complex; trifuran-2-yl-phosphane in tetrahydrofuran Stille coupling; Heating;
参考文献
Journal of the American Chemical Society, , vol. 125, # 50 p. 15292 - 15293
反应条件
PEPPSI™-IPr catalyst; cesium fluoride in 1,4-dioxane T=20 - 60°C; Stille-Migita cross-coupling; 24 h; Molecular sieveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 14 p. 4279 - 4283
反应条件
tris-(o-tolyl)phosphine; tris(dibenzylideneacetone)dipalladium (0) in N,N-dimethyl-formamide T=20°C; Stille reaction;
参考文献
Garcia-Cuadrado, Domingo; Cuadro, Ana M.; Alvarez-Builla, Julio; Vaquero, Juan Jose
Synlett, 2002 , # 11 p. 1904 - 1906