N,N-二乙基-3,4,5-三甲氧基苯甲酰胺合成路线 （共 8 条）
反应条件
Schwartz's reagent in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Leighty, Matthew W.; Spletstoser, Jared T.; Georg, Gunda I.
Organic Syntheses, 2012 , vol. 88, p. 427 - 437
反应条件
1: With disodium hydrogenphosphate in acetonitrile T=20°C; Methylation; 2: With sodium hydrogencarbonate Hydrolysis; 18 h;
参考文献
Tetrahedron, , vol. 56, # 51 p. 9875 - 9883
反应条件
in tetrahydrofuran
T=20°C; 0.5 h;
参考文献
Leighty, Matthew W.; Spletstoser, Jared T.; Georg, Gunda I.
Organic Syntheses, 2012 , vol. 88, p. 427 - 437
反应条件
1: oxalyl chloride / CH2Cl2; dimethylformamide / 2 h / Heating
2: pyridine / CH2Cl2 / 20 h
View Scheme
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
pyridine in dichloromethane
Substitution; 20 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
参考文献
Couturier
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 559,597
反应条件
oxalyl dichloride
1.) DMF, ether, ice cooling, 4 h, 2.) ether, ice cooling, 24 h; Yield givenMultistep reaction;
参考文献
Berg; Bladh
Acta chemica Scandinavica (Copenhagen, Denmark : 1989), 1998 , vol. 52, # 12 p. 1380 - 1385
参考文献
Couturier
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 559,597
