反应条件
1: 1) NaH / 1) DMF, 0 deg C, 3 h, 2) room temp., 36 h
2: pyridinium chlorochromate (PCC) / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
参考文献
Hashimoto, Masaru; Kan, Toshiyuki; Nozaki, Koji; Yanagiya, Mitsutoshi; Shirahama, Harushia; Matsumoto, Takeshi
Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5088 - 5107