O-(3,5-二甲氧基苯基)二甲基硫代氨基甲酸酯合成路线 （共 6 条）
反应条件
1: 100 percent / 6 h / 285 °C 2: 99 percent / KOH / methanol / Heating 3: 98 percent / KOH / 60 °C View Scheme
参考文献
Wolfers,H. et al.
Synthesis, 1975 , p. 43 - 44
反应条件
1: 100 percent / 6 h / 285 °C 2: 99 percent / KOH / methanol / Heating View Scheme
参考文献
Aquinox Pharmaceuticals Inc.
Patent: US2011/136802 A1, 2011 ;
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide
T=20°C;
参考文献
Aquinox Pharmaceuticals Inc.
Patent: US2011/136802 A1, 2011 ;
Location in patent: Page/Page column 16-17 ;
反应条件
1: 265 °C
2: aq. KOH / methanol
3: K2CO3 / acetone
4: aq. HI
View Scheme
参考文献
Wolfers,H. et al.
Synthesis, 1975 , p. 43 - 44
反应条件
T=285°C; Newman-Kwart rearrangement; 6 h;
参考文献
Aquinox Pharmaceuticals Inc.
Patent: US2011/136802 A1, 2011 ;
Location in patent: Page/Page column 16-17 ;
反应条件
1: 265 °C
2: aq. KOH / methanol
3: K2CO3 / acetone
4: aq. HI
View Scheme
参考文献
Wolfers,H. et al.
Synthesis, 1975 , p. 43 - 44
