2-(2-氨基苯硫基)-苯甲酸合成路线 (共 11 条)
参考文献
Polivka; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 5 p. 1465 - 1476
反应条件
trichlorophosphate 5 - 6 h; Heating / reflux; Product distribution / selectivity;
参考文献
JUBILANT ORGANOSYS LIMITED
Patent: WO2006/27789 A1, 2006 ;
Location in patent: Page/Page column 9; 15 ;
反应条件
1: 95 percent / polyphosphoric acid / 2 h / 140 °C 2: 65 percent / P2S5 / pyridine / 6.5 h / Heating View Scheme
参考文献
Polivka; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 5 p. 1465 - 1476
反应条件
ammonium hydroxide; iron(II) sulfate
参考文献
Mayer,F.
Chemische Berichte, 1909 , vol. 42, p. 3065
参考文献
Ube Industries, Ltd.
Patent: EP1201663 A1, 2002 ;
反应条件
1: 85 percent / Cu2O, pyridine / 3 h / Heating
2: ferrum reductum, iron(III) chloride / 1.) H2O, heating, 12 h, 2.) H2O, ethanol, heating, 5 h
View Scheme
参考文献
Kuti, M.; Rabai, J.; Kapovits, I.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 85, # 1-4 p. 119 - 128
反应条件
potassium hydroxide; copper
参考文献
Sindelar; Kakac; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1974 , vol. 39, # 1 p. 333 - 354
反应条件
1: 85 percent / Cu2O, pyridine / 3 h / Heating
2: ferrum reductum, iron(III) chloride / 1.) H2O, heating, 12 h, 2.) H2O, ethanol, heating, 5 h
View Scheme
参考文献
Kuti, M.; Rabai, J.; Kapovits, I.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 85, # 1-4 p. 119 - 128
反应条件
1: Reaktion ueber mehrere Stufen
2: ferrosulfate; aqueous ammonia
View Scheme
参考文献
Mayer,F.
Chemische Berichte, 1909 , vol. 42, p. 3065
反应条件
1: Reaktion ueber mehrere Stufen
2: ferrosulfate; aqueous ammonia
View Scheme
参考文献
Mayer,F.
Chemische Berichte, 1909 , vol. 42, p. 3065