1: 91 percent / toluene-p-sulphonic acid / benzene / 21 h / Heating
2: thionyl chloride / benzene / 30 h / Heating
3: 1.36 g / NaN3 / dimethylformamide / 4 h / Ambient temperature
4: 55 percent / light petroleum / 6 h / Irradiation
View Scheme
参考文献
Casey, Michael; Moody, Christopher; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1389 - 1394
1: 91 percent / toluene-p-sulphonic acid / benzene / 21 h / Heating
2: thionyl chloride / benzene / 30 h / Heating
3: 1.36 g / NaN3 / dimethylformamide / 4 h / Ambient temperature
4: 55 percent / light petroleum / 6 h / Irradiation
5: 89 percent / diethyl ether / 0.5 h
6: 1.) tBuOCl; 2.) DBU / 1.) ether, 4 h; 2.) 1 h
View Scheme
参考文献
Casey, Michael; Moody, Christopher; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1389 - 1394
1: 91 percent / toluene-p-sulphonic acid / benzene / 21 h / Heating
2: thionyl chloride / benzene / 30 h / Heating
3: 1.36 g / NaN3 / dimethylformamide / 4 h / Ambient temperature
View Scheme
参考文献
Casey, Michael; Moody, Christopher; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1389 - 1394
Mirskova, A. N.; Levkovskaya, G. G.; Drozdova, T. I.; Kalikhman, I. D.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 2 p. 397 - 398
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 452 - 453
