反应条件
triethylamine in dichloromethane byproducts: 1,2-dimethoxyethane; Slow addn. of solid W(C-t-Bu)Cl3(dme) to a stirred and cooled (-40°C) soln. of TIPTH and Et3N, soln. turns fisrt green, then red, warming (room temp.), stirring overnight.; Addn. of pentane, Et3NHCl pptd., filtn. through Celite, evapn. in vac. to dryness, elem. anal.;
参考文献
Murdzek, John S.; Blum, Lauren; Schrock, Richard R.
Organometallics, 1988 , vol. 7, p. 436 - 441
