2-叔丁氧羰基氨基丙烯酸甲酯合成路线 (共 79 条)
反应条件
in diethyl ether T=-60°C; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Bajgrowicz, J. A.; Hallaoui, A. El; Jacquier, R.; Pigiere, Ch.; Viallefont, Ph.
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2759 - 2762
反应条件
sodium hydride; sodium iodide 1. dimethoxyethane, -10 deg C -> room temp.; Yield given. Multistep reaction;
参考文献
Hermkens, Pedro H. H.; Maarseveen, Jan H. v.; Ottenheijm, Harry C. J.; Kruse, Chris G.; Scheeren, Hans W.
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 3998 - 4006
反应条件
in diethyl ether T=-60°C; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Bajgrowicz, J. A.; Hallaoui, A. El; Jacquier, R.; Pigiere, Ch.; Viallefont, Ph.
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2759 - 2762
反应条件
1: 93 percent / HMPA / tetrahydrofuran / 0.08 h / 0 °C 3: NaH / tetrahydrofuran / 0.05 h / 0 °C View Scheme
参考文献
Heterocycles, , vol. 44, # 1 p. 319 - 324
反应条件
2: NaH / tetrahydrofuran / 0.05 h / 0 °C View Scheme
参考文献
Heterocycles, , vol. 44, # 1 p. 319 - 324
参考文献
Organic and Biomolecular Chemistry, , vol. 3, # 13 p. 2476 - 2481
反应条件
1H-imidazole; iodine; triphenylphosphine
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 19, # 15 p. 4427 - 4431
反应条件
copper(l) iodide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -60 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845
反应条件
copper(l) iodide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -60 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845
反应条件
copper(l) iodide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -60 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845