La[N(TMS)2]3 in benzene-d6
T=60°C; Kinetics; Further Variations:Catalysts;
参考文献
Brinkmann, Christine; Barrett, Anthony G. M.; Reid, Stephanie; Hill, Michael S.; Procopiou, Panayiotis A.
Organometallics, 2012 , vol. 31, # 20 p. 7287 - 7297,11
copper (I) cyanide in tetrahydrofuran
under Ar or N2; the allene added to the Sn-Al compd. in THF followed by CuCN at -78°C, warmed to room temp. over 15h; hydrolyzed by addn. of MeOH, aq. NH4Cl, extn. (ether), flash chromy. (ethyl acetate : n-hexane = 1:9), elem. anal.;
参考文献
Singh, Shankar; Oehlshlager, Allan C.
Canadian Journal of Chemistry, 1991 , vol. 69, # 12 p. 1872 - 1880
