三-O-苄基-D-葡萄烯糖合成路线 (共 122 条)
反应条件
1: 2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl chloride With N,N-dimethylimidazolone; ethylene glycol dimethyl ether; nickel dichloride T=20°C; 0.333333 h; 2: (3-phenylpropyl)zinc(II) bromide 12 h;
参考文献
Journal of the American Chemical Society, , vol. 129, # 7 p. 1908 - 1909
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 1.5 h;
参考文献
Skrydstrup, Troels; Mazeas, Daniel; Elmouchir, Mohamed; Doisneau, Gilles; Riche, Claude; Chiaroni, Angele; Beau, Jean-Marie
Chemistry - A European Journal, 1997 , vol. 3, # 8 p. 1342 - 1356
反应条件
samarium diiodide; cyclohexanone in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Chemistry - A European Journal, , vol. 4, # 4 p. 655 - 671
反应条件
ethylene glycol dimethyl ether; nickel dichloride; Pybox in 1,3-dimethyl-imidazolidin-2-one; ethylene glycol dimethyl ether T=25°C; Negishi coupling reaction; 12 h;
参考文献
Journal of the American Chemical Society, , vol. 130, # 36 p. 12177 - 12183
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Skrydstrup, Troels; Jarreton, Olivier; Mazeas, Daniel; Urban, Dominique; Beau, Jean-Marie
Chemistry - A European Journal, 1998 , vol. 4, # 4 p. 655 - 671
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in tetrahydrofuran T=20°C; 3 h;
参考文献
Madhusudan, Soni Kamlesh; Agnihotri, Geetanjali; Negi, Devendra S.; Misra, Anup Kumar
Carbohydrate Research, 2005 , vol. 340, # 7 p. 1373 - 1377
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in tetrahydrofuran T=20°C; 3 h;
参考文献
Madhusudan, Soni Kamlesh; Agnihotri, Geetanjali; Negi, Devendra S.; Misra, Anup Kumar
Carbohydrate Research, 2005 , vol. 340, # 7 p. 1373 - 1377
反应条件
1: D-galactal With sodium hydride in N,N-dimethyl-formamide; oil T=0°C; 0.5 h; 2: benzyl chloride in N,N-dimethyl-formamide; oil T=20°C;
参考文献
Maiti, Dilip K.; Halder, Samiran; Pandit, Palash; Chatterjee, Nirbhik; De Joarder, Dripta; Pramanik, Nabyendu; Saima, Yasmin; Patra, Amarendra; Maiti, Prabir K.
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8086 - 8097
反应条件
sodium dihydrogenphosphate; zinc in ethyl acetate T=20°C; 3 h;
参考文献
Zhao, Jinzhong; Wei, Shanqiao; Ma, Xiaofeng; Shao, Huawu
Carbohydrate Research, 2010 , vol. 345, # 1 p. 168 - 171
反应条件
samarium diiodide in tetrahydrofuran T=20°C;
参考文献
Tetrahedron Letters, , vol. 38, # 10 p. 1767 - 1770