二溴硼烷二甲基硫醚络合物合成路线 （共 18 条）
反应条件
in carbon disulfide distn. (75°C/0.1 Torr);
参考文献
Gmelin Handbook: B: B Comp.SVol.1/3, 10.8.3, page 85 - 87
反应条件
1 h, 50°C; distn. (75°C/0.1 Torr);
参考文献
Gmelin Handbook: B: B Comp.SVol.1/3, 10.8.3, page 85 - 87
反应条件
dropwise addn. of BBr3 to the mixture of (CH3)2S*BH3 and (CH3)2S; 12 h mixing at 40°C;
参考文献
Inorganic Chemistry, , vol. 16, p. 2938 - 2940
反应条件
hydrogen bromide byproducts: H2;
参考文献
Z. Naturforsch. b, , vol. 30, p. 55 - 59
参考文献
Z. Naturforsch. b, , vol. 30, p. 55 - 59
反应条件
sodium hydroxide; dihydrogen peroxide directive effects in the hydroboration, isomer distribution; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 45, # 3 p. 384 - 389
反应条件
methanol in dichloromethane; pentane under N2, 1-hexene treated with BHBr2*SMe2 in CH2Cl2 followed by methanolysis in pentane at 0°C; distd.;
参考文献
Brown; Imai
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6285 - 6289
反应条件
sodium hydroxide; dihydrogen peroxide directive effects in the hydroboration, isomer distribution; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 45, # 3 p. 384 - 389
反应条件
water in dichloromethane (N2); addn. of HBBr2(SMe2) at 0°C; filtration after 12 h into mixture of ice and ether (1:1); stirring for 30 min at room temperature; washing of organic phase with satd. NaCl-soln.; drying (MgSO4); removal of solvent in vac.; washing with hexane;
参考文献
Bulletin de la Societe Chimique de France, , vol. 129, p. 554 - 565
反应条件
water in dichloromethane (N2); addn. of HBBr2(SMe2) at 0°C; filtration after 12 h into mixture of ice and ether (1:1); stirring for 30 min at room temperature; washing of organic phase with satd. NaCl-soln.; drying (MgSO4); removal of solvent in vac.; washing with hexane;
参考文献
Jego, J. M.; Carboni, B.; Vaultier, M.
Bulletin de la Societe Chimique de France, 1992 , vol. 129, p. 554 - 565
