copper(l) iodide; EtZnBr in neat (no solvent) CuI, Zn were placed in reactor, evacuated for 10 min, filled with Ar, ligand and EtZnBr were added, heated to 38-40°C for 4.5 h, cooled to room temp.; vac. distilled;
参考文献
Eremeev; Danov; Skudin; Sakhipov
Russian Journal of General Chemistry, 2003 , vol. 73, # 4 p. 556 - 559
in neat (no solvent) Sonication; (N2), ZnCl2 introduced into a flask connected to a condenser containingalcohol at -20°C, Et3Al (Et3Al/ZnCl2 2.2) dropped into flask over 10 min at room temp., stirred and heated at 100°C for 1 hed forfurther 20 min; distd.; NMR;
参考文献
Lin, Yih-tsung
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 277 - 284
in neat (no solvent) Sonication; (N2), ZnCl2 introduced into a flask connected to a condenser containingalcohol at -20°C, Et3Al*Et2O (Et3Al*Et2O/ZnCl2 2.6) dropped intoflask over 10 min at room temp., stirred and heated at 100°C for1 hed for further 20 min; distd.; NMR;
参考文献
Lin, Yih-tsung
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 277 - 284
