反应条件
in benzene byproducts: methyl acetate; under N2, soln. of EtZnOMe and CH3COOC(t-Bu)CH2 in C6H6 slowly heated to 60°C for 1 h; volatiles (methyl acetate, Et2Zn) removed, residue dissolved in pentane, cooled to -30°C;
参考文献
Dekker, Jan; Schouten, Abraham; Budzelaar, Peter H. M.; Boersma, Jaap; Van Der Kerk, Gerrit J. M.; et al.
Journal of Organometallic Chemistry, 1987 , vol. 320, p. 1 - 12
