1: 4-iodobenzoic acid ethyl ester; diethylzinc With t-Bu-N=P[N=P(NMe)3]3 in hexane; N,N-dimethyl-formamide T=20°C; 5 h; 2: iodobenzene With tetrakis(triphenylphosphine) palladium(0) in hexane; N,N-dimethyl-formamide T=20°C; Negishi coupling; 7 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ueno, Masahiro; Wheatley, Andrew E. H.; Kondo, Yoshinori
Chemical Communications, 2006 , # 33 p. 3549 - 3550
