Li in solid matrix
reaction of Li-atoms with CHBrX (e. g. CH2BrI) in Ar at 15K;; determination by IR;;
参考文献
Smith, D. W.; Andrews, L.
Journal of Chemical Physics, 1971 , vol. 55, p. 5295 - 5303
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Gmelin Handbook: C: MVol.D2, 3.18, page 89 - 90
Sm in tetrahydrofuran
to a mixt. of Sm powder and Ge compound (3:1) in THF added 3 equi. of CH2BrI at -78°C, warmed to room temp.; quenched (H2O), extd.(CH2Cl2) 3 times, dried (Na2SO4), evapd.(vac.), chromy.(silica gel);
参考文献
Kondo, Hitoshi; Yamanoi, Yoshinori; Nishihara, Hiroshi
Chemical Communications, 2011 , vol. 47, # 23 p. 6671 - 6673
