in benzene formation at treatment of a cold soln. of Sn(OC2H5)4 in benzene with excess CH3COF; boiling;; filtration of pptd. SnF4; washing with benzene and drying;;
参考文献
Yakubovich, A. A.; Makarov, S. P.; Ginsburg, V.
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 1006 - 1008
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 1036 - 1038
Full Text Show Details
Gmelin Handbook: Sn: MVol.C1, 5.6.1, page 171 - 172
Belen'kii,G.G.; German,L.S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1974 , vol. 23, # 4 p. 913 - 915
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1974 , vol. 23, # 4 p. 942 - 945
in toluene Mo2(O-i-Pr) was dissolved in a min. amt. of toluene. This soln. was cooled to -196°C. Acetyl fluorid was condensed into the react. vessel. The vessel was warmed to -20°C (2 d) and then cooled to -78°C. (7 d).; Filtration. Elem.anal.;
参考文献
Chisholm, Malcolm H.; Clark, David L.; Errington, R. John; Folting, Kirsten; Huffman, John C.
Inorganic Chemistry, 1988 , vol. 27, p. 2071 - 2084
