in neat (no solvent) mixture of 1 mol CBr4 and 4 mol Se; in a closed vessel at 250°C 20h;; distillation of Se2Br2 and small amount of CBr4, solid compound SeBr4, residue in flask: grey Se;;
参考文献
Briscoe; Peel; Rowlands
Journal of the Chemical Society, 1929 , p. 1766
Full Text Show Details
Gmelin Handbook: Se: MVol.A1, 79, page 254 - 257