3,3-二甲基-1-丁烯合成路线 （共 347 条）
反应条件
in benzene 0.5 h; Ambient temperatureIrradiation;
参考文献
Dicks, Patrick F.; Glover, Steohen A.; Goosen, Andre; McCleland, Cedric W.
Tetrahedron, 1987 , vol. 43, # 5 p. 923 - 934
反应条件
tetraethylammonium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dichloromethane T=20°C; 0.0833333 h; regioselective reaction;
参考文献
Deshmukh, Swapnil S.; Chaudhari, Kiran H.; Akamanchi, Krishnacharya G.
Synlett, 2011 , # 1 art. no. D18210ST, p. 81 - 83
反应条件
3-methyl-2-amino-pyridine; Wilkinson's catalyst; 1-Hexylamine; α,α,α-Trifluoro-p-toluic acid; water in toluene T=150°C; 24 h;
参考文献
Synlett, , # 18 p. 2939 - 2942
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 24 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
hydrogen; silica gel; ruthenium in gas T=200°C; 0.0833333 h; var. temp., var. contact time; Product distributionMechanism;
参考文献
Toyir, Jamil; Leconte, Michel; Niccolai, Gerald P.; Basset, Jean-Marie
Journal of Catalysis, 1995 , vol. 152, # 2 p. 306 - 312
反应条件
P=5 - 150 Torr; Ambient temperatureIrradiationpresence/absence of oxygen, DI; Quantum yield;
参考文献
Deslauriers, Helene; Collin, Guy J.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 62 - 67
反应条件
mercury(II) diacetate in tetrahydrofuran; water 1 h; Ambient temperatureother mercuri salts, other reaction time; Product distribution;
参考文献
Morrill, Terence C.; D'Souza, Christopher A.; Yang, Lu; Sampognaro, Anthony J.
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2481 - 2484
反应条件
oxygen; CoSMDPT var. reag.: H2O2, CH3COOH or K2O/18-crown-6; var. solv.; Product distribution;
参考文献
Hamilton, Dorothy E.; Drago, Russell S.; Zombeck, Alan
Journal of the American Chemical Society, 1987 , vol. 109, # 2 p. 374 - 379
反应条件
sodium hydroxide; sodium tetrahydroborate; Mercury(II) methanesulphonate 1.) THF/H2O, 15 min, room temp.; Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Geoghegan, Philip J.; Kurek, Joseph T.
Journal of Organic Chemistry, 1981 , vol. 46, # 19 p. 3810 - 3812
反应条件
sodium hydroxide; sodium tetrahydroborate; Hg(NO3)2 1.) 60 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brown, Herbert C.; Kurek, Joseph T.; Rei, Min-Hon; Thompson, Kerry L.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2551 - 2557
