3,3-二甲基-1-丁烯合成路线 （共 347 条）
反应条件
C18H32ClIrOP2S; sodium t-butanolate T=200°C; 1 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube; Reagent/catalystConcentrationTime;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., , vol. 126, # 5 p. 1414 - 1418
反应条件
potassium permanganate
参考文献
Claessens
Bulletin de la Societe Chimique de France, 1909 , vol. <4>5, p. 114
Full Text Show Details
Fomin; Sochanski
Chemische Berichte, 1913 , vol. 46, p. 247
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 12 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
polyethylene glycol-400; water; oxygen; palladium dichloride T=65°C; P=10343 Torr;
参考文献
Alper, Howard; Januszkiewicz, Krysztof; Smith, David J. H.
Tetrahedron Letters, 1985 , vol. 26, # 19 p. 2263 - 2264
反应条件
oxygen in benzene benzene, 25°C, 120 h, air;; evapn.; flash chromy. on silica gel;;
参考文献
Organometallics, , vol. 3, p. 1777 - 1785
反应条件
oxygen; CoSMDPT var. reag.: H2O2, CH3COOH or K2O/18-crown-6; var. solv.; Product distribution;
参考文献
Hamilton, Dorothy E.; Drago, Russell S.; Zombeck, Alan
Journal of the American Chemical Society, 1987 , vol. 109, # 2 p. 374 - 379
反应条件
dimethylsulfide borane complex; pyridinium chlorochromate 1.) CH2Cl2, 1 h, RT; 2.) CH2Cl2, reflux, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brown, Herbert C.; Kulkarni, Surendra U.; Rao, C. Gundu; Patil, Vemanna D.
Tetrahedron, 1986 , vol. 42, # 20 p. 5515 - 5522
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 12 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
IrH2{C6H3-2,6-(CH2PBu(t)2)2} in 1,3,5-trimethyl-benzene T=55°C; Kinetics;
参考文献
Renkema, Kenton B.; Kissin, Yury V.; Goldman, Alan S.
Journal of the American Chemical Society, 2003 , vol. 125, # 26 p. 7770 - 7771
反应条件
cephaloridine T=160 - 170°C;
参考文献
Delacre
Chem. Zentralbl., 1906 , vol. 77, # II p. 498
