3,3-二甲基-1-丁烯合成路线 (共 347 条)
反应条件
anhydrous aluminium sulphate T=275°C;
参考文献
Shell Devel. Co.
Patent: US2217252 , 1938 ;
反应条件
boron trifluoride in diethyl ether T=25°C; 3 h;
参考文献
Brooke, Gerald M.; Cooperwaite, John R.; Morpeth, Alan G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2637 - 2642
反应条件
zinc(II) chloride in diethyl ether 22 h; Heating; Yield given. Yields of byproduct given;
参考文献
Brooke, Gerald M.; Cooperwaite, John R.; Morpeth, Alan G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2637 - 2642
反应条件
aluminum oxide; {4-OK-C6H2-2,6-[OP(t-Bu)2]2}Ir(C2H4) 2.96667 h; Heating; Product distribution / selectivity;
参考文献
THE UNIVERSITY OF NORTH CAROLINA AT CHAPEL HILL
Patent: WO2008/153869 A2, 2008 ;
Location in patent: Page/Page column 19-20 ;
反应条件
aluminum oxide; {4-OK-C6H2-2,6-[OP(t-Bu)2]2}Ir(C2H4) 39.9667 h; Heating; Product distribution / selectivity;
参考文献
THE UNIVERSITY OF NORTH CAROLINA AT CHAPEL HILL
Patent: WO2008/153869 A2, 2008 ;
Location in patent: Page/Page column 19-20 ;
反应条件
aluminum oxide; C24H42IrO3P2(1-)*K(1+) T=200°C; 40 h; Inert atmosphere; Kinetics; Reagent/catalystTemperatureTime;
参考文献
Huang, Zheng; Brookhart, Maurice; Goldman, Alan S.; Kundu, Sabuj; Ray, Amlan; Scott, Susannah L.; Vicente, Brian C.
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 1-2 p. 188 - 206
参考文献
Lebedew; Kudrjawzew
Zhurnal Obshchei Khimii, 1935 , vol. 5, p. 1861
Chem. Zentralbl., 1936 , vol. 107, # I p. 3818
反应条件
T=400°C; Isomerisierung und Fragmentierung; Produkt5: Propen;
参考文献
Obolenzew; Grjasew
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 1588,1594,1596;engl.Ausg.S.1741
参考文献
Delacre
Chem. Zentralbl., 1906 , vol. 77, # II p. 498
反应条件
in dichloromethane; benzene T=14 - 15°C; Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 104, # 25 p. 7267 - 7274