3,3-二甲基-1-丁烯合成路线 (共 347 条)
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=200°C; 24 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=200°C; 24 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
(η5-C5Me5)Rh(H)2(SiEt3)2 in cyclohexane T=150°C; 12 h; var. of catalyst, hydrogen acceptor, ratio, time; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 16 p. 1897 - 1898
反应条件
T=300°C; P=7355.08 Torr; Hydrogenation;
参考文献
Pines et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 6390
反应条件
[(2,6-C6H3(CH2P(CF3)2)2)Ir(.eta.4-cyclooctadiene)] T=150°C; 48 h;
参考文献
Adams, Jeramie J.; Arulsamy, Navamoney; Roddick, Dean M.
Organometallics, 2012 , vol. 31, # 4 p. 1439 - 1447
反应条件
IrH5P2 T=30°C; 0.833333 h; study of transfer hydrogenation; Product distribution;
参考文献
Goldman, Alan S.; Halpern, Jack
Journal of the American Chemical Society, 1987 , vol. 109, # 24 p. 7537 - 7539
反应条件
T=180°C; 1 h; Reagent/catalystTime;
参考文献
Kundu, Sabuj; Lyons, Thomas W.; Brookhart, Maurice
ACS Catalysis, 2013 , vol. 3, # 8 p. 1768 - 1773
反应条件
aluminum oxide; {4-OK-C6H2-2,6-[OP(t-Bu)2]2}Ir(C2H4) 2.96667 h; Heating; Product distribution / selectivity;
参考文献
THE UNIVERSITY OF NORTH CAROLINA AT CHAPEL HILL
Patent: WO2008/153869 A2, 2008 ;
Location in patent: Page/Page column 19-20 ;
反应条件
C18H32ClIrOP2S; sodium t-butanolate T=100°C; 4 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
C18H32ClIrOP2S; sodium t-butanolate T=200°C; 1 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube; Reagent/catalystConcentrationTime;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418