1: With vilsmeier reagent in isobutyramide; N,N-dimethyl-formamide T=3 - 105°C; 2: With water; sodium hydroxide in isobutyramide; N,N-dimethyl-formamide T=20°C; pH=9.75; Product distribution / selectivity;
参考文献
TATE and LYLE TECHNOLOGY LIMITED; WILEY, James, Edwin; JABER, Mohamad, R.
Patent: WO2010/151489 A1, 2010 ;
Location in patent: Page/Page column 14 ;
1: With N-(chloromethylene)-N-methylmethanaminium chloride T=85 - 115°C; 6.5 h; 2: With sodium hydroxide in water pH=9.0; 4 - 5 h; Product distribution / selectivity;
