2-苯并噻唑-2-基-1-苯乙酮合成路线 （共 9 条）
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; bis(1,2-diphenylphosphino)benzene in chlorobenzene 6 h; Inert atmosphereReflux;
参考文献
Li, Guangzhe; Arisawa, Mieko; Yamaguchi, Masahiko
Chemical Communications, 2014 , vol. 50, # 33 p. 4328 - 4330
反应条件
0.0833333 h; Heating;
参考文献
Ciurdaru,G.; Ciuciu,M.
Journal fuer Praktische Chemie (Leipzig), 1979 , vol. 321, p. 320 - 322
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; bis(1,2-diphenylphosphino)benzene in chlorobenzene Inert atmosphereReflux;
参考文献
Li, Guangzhe; Arisawa, Mieko; Yamaguchi, Masahiko
Chemical Communications, 2014 , vol. 50, # 33 p. 4328 - 4330
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; bis(1,2-diphenylphosphino)benzene in chlorobenzene Inert atmosphereReflux;
参考文献
Li, Guangzhe; Arisawa, Mieko; Yamaguchi, Masahiko
Chemical Communications, 2014 , vol. 50, # 33 p. 4328 - 4330
反应条件
1: 2-Methyl-benzothiazole With n-butyllithium in tetrahydrofuran; cyclohexane
T=-70°C; 1.5 h;
2: benzoic acid ethyl ester T=-70°C; 1.5 h;
3: in methanol
参考文献
KINETEK PHARMACEUTICALS, INC.
Patent: WO2004/11460 A2, 2004 ;
Location in patent: Page 99 ;
WO 2004/011460 A2
反应条件
in diethyl ether
1) -78 deg C, 1 h, 2) to 0 deg C;
参考文献
Costa, Maria Virginia; Brembilla, Alain; Roizard, Denis; Lochon, Pierre
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 6 p. 1541 - 1544
反应条件
1: phenyllithium / benzene; diethyl ether / -78 °C
2: 51 percent / diethyl ether / 1) -78 deg C, 1 h, 2) to 0 deg C
View Scheme
参考文献
Costa, Maria Virginia; Brembilla, Alain; Roizard, Denis; Lochon, Pierre
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 6 p. 1541 - 1544
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; bis(1,2-diphenylphosphino)benzene in chlorobenzene
6 h; Inert atmosphereReflux;
参考文献
Li, Guangzhe; Arisawa, Mieko; Yamaguchi, Masahiko
Chemical Communications, 2014 , vol. 50, # 33 p. 4328 - 4330
反应条件
(i) (heating), (ii) Py; Multistep reaction;
参考文献
Barnikow,G.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1966 , vol. 6, p. 109 - 110
