反应条件
1: 1.) Mg, 2.) NH4Cl / 1.) ether, reflux, 24 h, 2.) H2O, 0 deg C, 30 min 2: 1.) H2, 2.) HCl, 3.) NaNO2, 4.) LiAlH4, 5.) tert-butyl hypochlorite, Et3N 3: 44 percent / CCl3F / 0 °C / 1.) -78 deg C, direct photolyses, CFCl3; 2.) -78 deg C, sensitized photolyses View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 24 p. 6660 - 6668
