1: With phenyltrimethyl silane; C69H55ClP3Ru in tetrahydrofuran
T=60°C; 16 h; Glovebox;
2: With hydrogenchloride in tetrahydrofuran; water
T=20°C; 1 h; Glovebox; chemoselective reaction;
参考文献
Fernandez-Salas, Jose A.; Manzini, Simone; Nolan, Steven P.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 308 - 312
Lee, Chih-Hung; Perner, Richard J.; Larson, Daniel P.; Koenig, John R.; Gomtsyan, Arthur R.; Zheng, Guo Zhu; DiDomenico, Stanley; Stewart, Andrew O.; Bayburt, Erol K.
Patent: US2002/173665 A1, 2002 ;
US 20020173665 A1