3,4-二苯基-5H-呋喃-2-酮合成路线 (共 40 条)
反应条件
potassium fluoride; tris(dibenzylideneacetone)dipalladium (0); tris-(o-tolyl)phosphine in toluene
T=85°C; 24 h;
参考文献
Bellina, Fabio; Anselmi, Chiara; Martina, Francesca; Rossi, Renzo
European Journal of Organic Chemistry, 2003 , # 12 p. 2290 - 2302
反应条件
water; PtCl4-CO in tetrahydrofuran
T=80°C; P=1034.3 Torr; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Baidossi, Wael; Lahav, Michal; Blum, Jochanan
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 669 - 672
反应条件
copper(l) iodide; triphenyl-arsane; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=80°C; Stille coupling; 24 h;
参考文献
Carter, Neil B.; Mabon, Ross; Walmsley, Rachel; Richecur, Alexandre M. E.; Sweeney
Synlett, 2006 , # 11 p. 1747 - 1749
反应条件
lithium aluminium tetrahydride in diethyl ether
T=-20°C; 0.75 h;
参考文献
Urove, Greg A.; Welker, Mark E.; Eaton, Bruce E.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 105 - 114
反应条件
PCy3; palladium diacetate; sodium hydrogencarbonate in methanol
T=60°C; 3 h; Inert atmosphere;
参考文献
Bellina, Fabio; Marchetti, Chiara; Rossi, Renzo
European Journal of Organic Chemistry, 2009 , # 27 p. 4685 - 4690
反应条件
PPh3 gold(I) chloro complex; silver trifluoromethanesulfonate in dichloromethane
T=25°C; 2 h;
参考文献
Bauer, Juergen T.; Hadfield, Maximillian S.; Lee, Ai-Lan
Chemical Communications, 2008 , # 47 p. 6405 - 6407
反应条件
calcium hydroxide powder; methyl iodide; dicobalt octacarbonyl in methanol; water
T=20°C; 20 h;
参考文献
Miura, Masahiro; Okuro, Kazumi; Hattori, Ayako; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 73 - 76
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=0°C; 0.0833333 h;
参考文献
Ji, Kegong; Zhao, Yulong; Zhang, Liming
Angewandte Chemie - International Edition, 2013 , vol. 52, # 25 p. 6508 - 6512
Angew. Chem., 2013 , vol. 125, # 25 p. 6636 - 6640
反应条件
PPh3 gold(I) chloro complex; silver trifluoromethanesulfonate in dichloromethane
T=20°C; 1 h;
参考文献
Li, Changkun; Zeng, Yi; Wang, Jianbo
Tetrahedron Letters, 2009 , vol. 50, # 24 p. 2956 - 2959
反应条件
tris(dibenzylideneacetone)dipalladium (0); tris-(o-tolyl)phosphine in 1-methyl-pyrrolidin-2-one
T=85°C;
参考文献
Bellina, Fabio; Anselmi, Chiara; Rossi, Renzo
Tetrahedron Letters, 2002 , vol. 43, # 11 p. 2023 - 2027