3,4-二苯基-5H-呋喃-2-酮合成路线 (共 40 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in benzene
T=100°C; 0.5 h; Microwave irradiation;
参考文献
Reddy, Maddi Sridhar; Thirupathi, Nuligonda; Hari Babu, Madala; Puri, Surendra
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 5878 - 5888
反应条件
hydrogenchloride in chloroform
1 h; Ambient temperature;
参考文献
Toda, Fumio; Takehira, Yoshikazu; Kataoka, Yutaka; Mori, Koji; Sato, Tamie; Segawa, Mari
Journal of the Chemical Society, Chemical Communications, 1984 , # 18 p. 1234 - 1235
反应条件
triethylamine in acetonitrile
Heating;
参考文献
Ahluwalia, V. K.; Mehta, Bhupinder; Kumar, Rakesh
Synthetic Communications, 1989 , vol. 19, # 3and4 p. 619 - 626
反应条件
hydrogen; dodecacarbonyltetrarhodium(0)
参考文献
Doyama, Kazuo; Joh, Takashi; Takahashi, Shigetoshi
Tetrahedron Letters, 1986 , vol. 27, # 37 p. 4497 - 4500
反应条件
1: 65 percent / aluminium isopropoxide / propan-2-ol / 6 h / Heating; solvent gradually distilled away
2: 37 percent / methyl iodide, Ca(OH)2 / Co2(CO)8 / methanol; H2O / 20 h / 20 °C
View Scheme
参考文献
Miura, Masahiro; Okuro, Kazumi; Hattori, Ayako; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 73 - 76
反应条件
2: TiCl4 / CH2Cl2 / -78 °C
3: DBU / toluene / 60 °C
View Scheme
参考文献
Demnitz, F. W. J.
Tetrahedron Letters, 1989 , vol. 30, # 45 p. 6109 - 6112
反应条件
calcium hydroxide powder; carbon monoxide; methyl iodide in methanol; water
20°C, 20 h.;
参考文献
Miura, Masahiro; Okuro, Kazumi; Hattori, Ayako; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 73 - 76
反应条件
1: TiCl4 / CH2Cl2 / -78 °C
2: DBU / toluene / 60 °C
View Scheme
参考文献
Demnitz, F. W. J.
Tetrahedron Letters, 1989 , vol. 30, # 45 p. 6109 - 6112
反应条件
1: TiCl4 / CH2Cl2 / -78 °C
2: DBU / toluene / 60 °C
View Scheme
参考文献
Demnitz, F. W. J.
Tetrahedron Letters, 1989 , vol. 30, # 45 p. 6109 - 6112
反应条件
copper(l) iodide; Pd(dppb)2; triphenyl-arsane in tetrahydrofuran
T=50°C; Stille reaction; Product distribution; Further Variations:ReagentsSolventsTemperaturesreaction times;
参考文献
Carter, Neil B; Mabon, Ross; Richecur, Alexandre M.E; Sweeney
Tetrahedron, 2002 , vol. 58, # 44 p. 9117 - 9129