2,6,6-三甲基环己-2-烯-1-羧酸合成路线 (共 37 条)
参考文献
Bougault
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1910 , vol. 150, p. 397
反应条件
phosphoric acid in toluene
T=100°C; Cyclization; 2 h;
参考文献
Gan, Yonghong; Li, Anpai; Pan, Xinfu; Chan, Albert S. C.; Yang, Teng-Kuei
Tetrahedron Asymmetry, 2000 , vol. 11, # 3 p. 781 - 787
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Yonghong, Gan; Xinfu, Pan
Journal of Chemical Research - Part S, 2000 , # 3 p. 130 - 132
反应条件
phosphoric acid in toluene
T=100°C; 2 h;
参考文献
Kron, A. A.; Burdin, E. A.; Novikov, N. A.; Aul'chenko, I. S.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1901 - 1904
Zhurnal Organicheskoi Khimii, 1990 , vol. 27, # 10 p. 2149 - 2154
反应条件
sulfuric acid in nitromethane
T=-40°C; 1 h;
参考文献
Lyashchuk, S. N.; Skrypnik, Yu. G.; Bezrodnyi, B. P.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.2 p. 109 - 114
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 1 p. 130 - 136
反应条件
formic acid
0.333333 h; Heating; Yields of byproduct given;
参考文献
Kadas, Istvan; Arvai, Geza; Horyath, Gabriella
Organic Preparations and Procedures International, 1998 , vol. 30, # 1 p. 79 - 85
反应条件
potassium permanganate; potassium carbonate in isopropyl alcohol
T=20°C; 5 h;
参考文献
Qianchao; Shiqing, Pi; Xinzhi, Chen
Journal of Chemical Research, 2007 , # 8 p. 494 - 496
反应条件
boron trifluoride diethyl etherate; acetic acid in toluene
T=0 - 25°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Armstrong, Rosemary J.; Weiler, Larry
Canadian Journal of Chemistry, 1983 , vol. 61, p. 2530 - 2539
反应条件
potassium hydroxide
T=110 - 120°C; im Autoklaven;
参考文献
Bouveault
Bulletin de la Societe Chimique de France, 1910 , vol. <4> 7, p. 354
反应条件
H2O in water; acetonitrile
T=25°C; 88 h; var. pH and μ, other solvent; Product distributionRate constant;
参考文献
Allen, Annette D.; Stevenson, Andrew; Tidwell, Thomas T.
Journal of Organic Chemistry, 1989 , vol. 54, # 12 p. 2843 - 2848
反应条件
Rexyn 201 (OH form) in methanol
Yield given. Yields of byproduct given;
参考文献
Frank, Arlen W.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 549 - 554