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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
56421-85-3
合成路线
（共 11 条）
5332-24-1
3-溴喹啉
+
6165-69-1
3-噻吩硼酸
→
反应条件
56421-85-3
反应条件
potassium phosphate; C52H66NO3PPdS in tetrahydrofuran; water T=20°C; Suzuki-Miyaura Coupling; 0.5 h; Sealed tubeInert atmosphere; Reagent/catalyst;
参考文献
Bruno, Nicholas C.; Niljianskul, Nootaree; Buchwald, Stephen L.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4161 - 4166
17249-80-8
3-氯噻吩
+
191162-39-7
喹啉-3-硼酸
→
反应条件
56421-85-3
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst; tetrabutylammomium bromide in 1-methyl-pyrrolidin-2-one; water; toluene T=90°C; Suzuki-Miyaura cross-coupling; Continuous flow reactorInert atmosphere;
参考文献
Noel, Timothy; Musacchio, Andrew J.
Organic Letters, 2011 , vol. 13, # 19 p. 5180 - 5183
5332-24-1
3-溴喹啉
→
反应条件
56421-85-3
反应条件
palladium diacetate; tris-(o-tolyl)phosphine in toluene T=20°C; 5 h; Inert atmosphere;
参考文献
Chen, Xu; Zhou, Lingmin; Li, Yimei; Xie, Tao; Zhou, Shuangliu
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 230 - 239
5332-24-1
3-溴喹啉
+
70161-87-4
→
反应条件
56421-85-3
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in 1,4-dioxane 16 h; Heating;
参考文献
Maguire, Martin P.; Sheets, Kimberly R.; McVety, Karen; Spada, Alfred P.; Zilberstein, Asher
Journal of Medicinal Chemistry, 1994 , vol. 37, # 14 p. 2129 - 2137
10486-61-0
3-碘噻吩
+
1207760-36-8
→
反应条件
56421-85-3
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 1 h; Inert atmosphere;
参考文献
Kim, Seung-Hoi; Rieke, Reuben D.
Tetrahedron, 2010 , vol. 66, # 17 p. 3135 - 3146
872-31-1
3-溴噻吩
+
5332-24-1
3-溴喹啉
→
反应条件
56421-85-3
反应条件
1: 3-(bromo)-quinoline With (nBu)3MgLi in tetrahydrofuran; diethyl ether; hexane T=-30 - -10°C; 2: thien-3-yl bromide With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; diethyl ether; hexane T=-10 - 20°C; 19 h;
参考文献
Dumouchel, Sylvain; Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Tetrahedron, 2003 , vol. 59, # 43 p. 8629 - 8640
872-31-1
3-溴噻吩
→
反应条件
56421-85-3
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [Pd2(dba)2] in tetrahydrofuran T=20°C; 18 h;
参考文献
Dumouchel, Sylvain; Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Tetrahedron Letters, 2003 , vol. 44, # 19 p. 3877 - 3880
5332-24-1
3-溴喹啉
+
214360-70-0
噻吩-3-硼酸频哪醇酯
→
反应条件
56421-85-3
反应条件
tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; toluene Suzuki cross-coupling; Heating;
参考文献
Miura, Masanori; Koike, Takanori; Ishihara, Tsukasa; Sakamoto, Shuichi; Okada, Minoru; Ohta, Mitsuaki; Tsukamoto, Shin-Ichi
Synthetic Communications, 2007 , vol. 37, # 5 p. 667 - 674
10486-61-0
3-碘噻吩
+
5332-24-1
3-溴喹啉
→
反应条件
56421-85-3
反应条件
1: 3-(bromo)-quinoline With lithium chloride; zinc in tetrahydrofuran 2 h; Inert atmosphereReflux; 2: 3-iodothiophene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 1 h; Inert atmosphere;
参考文献
Kim, Seung-Hoi; Slocum, Tim B.; Rieke, Reuben D.
Synthesis, 2009 , # 22 art. no. M02609SS, p. 3823 - 3827
188290-36-0
+
580-17-6
3-氨基喹啉
→
反应条件
59321-69-6
+
56421-85-3
反应条件
isopentyl nitrite T=70 - 80°C;
参考文献
Vernin,G.; Metzger,J.
Journal of Organic Chemistry, 1975 , vol. 40, p. 3183 - 3189
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