2-氧代-3-苯基-丙醛合成路线 (共 20 条)
反应条件
(PhO)3PO3 in dichloromethane
T=-15°C; various diazocompounds, oxidation; Product distributionMechanismRate constant;
参考文献
Shereshovets, V. V.; Korotaeva, N. M.; Vorob'ev, A. S.; Komissarov, V. D.; Furlei, I. I.
Russian Chemical Bulletin, 1994 , vol. 43, # 9 p. 1479 - 1483
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 9 p. 1567 - 1571
反应条件
2: aq. H3PO4
View Scheme
参考文献
Dahn,H. et al.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1000 - 1006
参考文献
Rioux-Lacoste,C.; Viel,C.
Bulletin de la Societe Chimique de France, 1974 , p. 2463 - 2470
参考文献
Bennett; Willis
Journal of the Chemical Society, 1928 , p. 1974
Journal of the Chemical Society, 1930 , p. 1709
Full Text Show Details
Dakin; Dudley
Journal of Biological Chemistry, 1914 , vol. 18, p. 38
Journal of the Chemical Society, 1914 , vol. 105, p. 2461
反应条件
Behandeln des Reaktionsprodukts mit Ammoniumchlorid-Loesung und Kochen des entstandenen Diaethylacetals mit verd. Schwefelsaeure;
参考文献
Dakin; Dudley
Journal of Biological Chemistry, 1914 , vol. 18, p. 38
Journal of the Chemical Society, 1914 , vol. 105, p. 2461
反应条件
diethyl ether; etheric solution
Behandeln des Reaktionsprodukts mit verd. wss. Schwefelsaeure;
参考文献
Bradley; Eaton
Journal of the Chemical Society, 1937 , p. 1913
反应条件
1: in ethanol
0.333333 h; Inert atmosphere;
2: With hydrogenchloride in ethanol; water
18 h; Reflux;
参考文献
Promega Corporation
Patent: US7692022 B2, 2010 ;
Location in patent: Page/Page column 46 ;
US 7692022 B2
反应条件
pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol
T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Jin, Shiow-Jen; Arora, Pramod K.; Sayre, Lawrence M.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3011 - 3018
反应条件
pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol
T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Jin, Shiow-Jen; Arora, Pramod K.; Sayre, Lawrence M.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3011 - 3018
反应条件
pyridine; oxygen; triethylamine; pyridine; compound with copper (II)-nitrate in methanol
T=25°C; P=1748 Torr; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Jin, Shiow-Jen; Arora, Pramod K.; Sayre, Lawrence M.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3011 - 3018