4-甲基-1-戊炔-3-醇合成路线 （共 30 条）
参考文献
Chemische Berichte, , vol. 60, p. 1872
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 59, p. 1145
参考文献
Chemische Berichte, , vol. 60, p. 1868
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 59, p. 1138
反应条件
palladium 10 on activated carbon; hydrogen in pentane optical yield given as percent ee;
参考文献
Mori, Kenji; Tashiro, Takuya
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3266 - 3269
反应条件
1: palladium/calcium carbonate / Hydrogenation 2: aluminium phosphate / 300 - 310 °C 3: zirconium (IV)-oxide /pumice stone / 300 - 310 °C View Scheme
参考文献
Nasarow; Mawrow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 472,482; engl. Ausg. S. 446, 454
反应条件
sodium acetate; copper dichloride; palladium dichloride T=12 - 13°C; 1.5 h;
参考文献
Trofimov; Mal'kina; Gritsa; Skvortsov; Stankevich; Sokolyanskaya
Russian Journal of General Chemistry, 1996 , vol. 66, # 1 p. 102 - 106
反应条件
copper(l) iodide; sodium carbonate; bis-triphenylphosphine-palladium(II) chloride in 1,4-dioxane Heating;
参考文献
Ivanchikova, Irena D.; Lebedeva, Nadezhda I.; Shvartsberg, Mark S.
Synthesis, 2004 , # 13 p. 2131 - 2134
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine; lithium chloride in N,N-dimethyl-formamide T=120°C; Larock Annulation; 16 h;
参考文献
Wang, Christy; Sperry, Jonathan
Tetrahedron, 2013 , vol. 69, # 23 p. 4563 - 4577
反应条件
1.1: triethylamine / dichloromethane / 20 °C 2.1: 2,6-bis[(4S)-4-methyl-4,5-dihydrooxazol-2-yl]pyridine; copper(l) iodide / methanol / 18 - 25 °C 2.2: 24 h / 18 - 25 °C 3.1: [bis(acetoxy)iodo]benzene / methanol; acetonitrile / 2.5 h / 20 °C 3.2: 1.5 h 4.1: potassium carbonate / dichloromethane / 17 h / 20 °C / pH 11 View Scheme
参考文献
Detz, Remko J.; Abiri, Zohar; Le Griel, Remi; Hiemstra, Henk; Van Maarseveen, Jan H.
Chemistry - A European Journal, 2011 , vol. 17, # 21 p. 5921 - 5930
反应条件
(i) SOCl2, (ii) Zn-Cu, ethane-1,2-diol, cyclohexanol; Multistep reaction;
参考文献
Pasto, Daniel J.; Warren, Steven E.; Morrison, Marjorie A.
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2837 - 2841
反应条件
Jone's reagent in acetone
参考文献
Mori, Kenji; Tashiro, Takuya; Zhao, Boguang; Suckling, David M.; El-Sayed, Ashraf M.
Tetrahedron, 2010 , vol. 66, # 14 p. 2642 - 2653
