2,4-二甲基-3-戊酮合成路线 （共 349 条）
反应条件
toluene-4-sulfonic acid in benzene 20 h; Heating;
参考文献
Yu; Bronson; Yang; Patick; Alam; Brankovan; Datema; Hitchcock; Martin
Journal of Medicinal Chemistry, 1993 , vol. 36, # 19 p. 2726 - 2738
反应条件
trimethylhexadecylammonium chloride; calcium carbonate; CaO in 1,4-dioxane T=25°C; 5 h; Sonication;
参考文献
Pazdera, Pavel; Simbera, Jan
Organic Preparations and Procedures International, 2011 , vol. 43, # 3 p. 297 - 301
反应条件
1: 1.) NaNH2 / 1.) toluene; 2.) toluene 2: 98 percent / LiBr / diethyl ether 3: 94 percent / SOCl2 / pyridine View Scheme
参考文献
Whitmore; Laughlin
Journal of the American Chemical Society, 1933 , vol. 55, p. 3736
反应条件
1: 2,4-dimethylpentan-3-one With lithium diisopropyl amide in tetrahydrofuran; n-heptane T=0°C; 1 h; 2: benzyl bromide in tetrahydrofuran; n-heptane T=0 - 50°C;
参考文献
FIRMENICH SA
Patent: WO2005/110961 A1, 2005 ;
Location in patent: Page/Page column 9 ;
参考文献
Cornforth,D.A. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2799 - 2805
反应条件
oxygen in decane T=49.9 - 99.9°C; Irradiationtime interval - 900-7200 s; Product distributionMechanismKinetics;
参考文献
Costello, Andrew R.; Lindsay Smith, John R.; Waddington, David J.
International Journal of Chemical Kinetics, 1996 , vol. 28, # 3 p. 201 - 215
反应条件
1: 4-tert-butyl-4-hydroxy-2,2,5,5-tetramethylhexan-3-one With n-butyllithium in hexane; pentane T=-40°C; 2: 2,4-dimethylpentan-3-one in hexane; pentane T=-40 - 20°C;
参考文献
Knorr; Boehrer; Schubert
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7506 - 7515
反应条件
sodium amide; benzene
参考文献
Bhatia et al.
Journal of the Chemical Society, 1959 , p. 24,28
反应条件
sodium amide; benzene
参考文献
Haller; Bauer
Annales de Chimie (Cachan, France), 1924 , vol. <10>1, p. 292
反应条件
und beim Behandeln des entstehenden Natriumverbindung mit Methyljodid in Benzol;
参考文献
Haller; Bauer
Annales de Chimie (Cachan, France), 1924 , vol. <10>1, p. 292
