1: 4-methoxy-aniline With triethylamine in dichloromethane
0.166667 h; Inert atmosphereCooling with ice;
2: pivaloyl chloride in dichloromethane
T=25°C; Inert atmosphereCooling with ice;
参考文献
Medina-Ramos, Wilmarie; Mojica, Mike A.; Cope, Elizabeth D.; Hart, Ryan J.; Pollet, Pamela; Eckert, Charles A.; Liotta, Charles L.
Green Chemistry, 2014 , vol. 16, # 4 p. 2147 - 2155
1.1: water / 6.67 h / 275 °C / |Inert atmosphere
2.1: triethylamine / dichloromethane / 0.17 h / |Inert atmosphere; |Cooling with ice
2.2: 25 °C / |Inert atmosphere; |Cooling with ice
View Scheme
参考文献
Medina-Ramos, Wilmarie; Mojica, Mike A.; Cope, Elizabeth D.; Hart, Ryan J.; Pollet, Pamela; Eckert, Charles A.; Liotta, Charles L.
Green Chemistry, 2014 , vol. 16, # 4 p. 2147 - 2155
1.1: water / 150 °C / |Green chemistry
2.1: water / 150 °C / |Green chemistry
3.1: triethylamine / dichloromethane / 0.17 h / |Inert atmosphere; |Cooling with ice
3.2: 25 °C / |Inert atmosphere; |Cooling with ice
View Scheme
参考文献
Medina-Ramos, Wilmarie; Mojica, Mike A.; Cope, Elizabeth D.; Hart, Ryan J.; Pollet, Pamela; Eckert, Charles A.; Liotta, Charles L.
Green Chemistry, 2014 , vol. 16, # 4 p. 2147 - 2155
1.1: water / 150 °C / |Green chemistry
2.1: triethylamine / dichloromethane / 0.17 h / |Inert atmosphere; |Cooling with ice
2.2: 25 °C / |Inert atmosphere; |Cooling with ice
View Scheme
参考文献
Medina-Ramos, Wilmarie; Mojica, Mike A.; Cope, Elizabeth D.; Hart, Ryan J.; Pollet, Pamela; Eckert, Charles A.; Liotta, Charles L.
Green Chemistry, 2014 , vol. 16, # 4 p. 2147 - 2155
